Synthesis, Spectral Analysis and Antimicrobial Activity of New Pd(II) Complexes Involving 5,6-Dimethylbenzimidazole

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dc.contributor.authorTurkyilmaz, Murat
dc.contributor.authorDonmez, Murat
dc.contributor.authorAltun, Ozlen
dc.date.accessioned2024-06-12T11:09:12Z
dc.date.available2024-06-12T11:09:12Z
dc.date.issued2023
dc.departmentTrakya Üniversitesien_US
dc.description.abstractIn this study, firstly, 3-bromopropanenitrile(2a), ethyl bromoacetate(2b), and 2-bromoethan-1-amine(2c) were added to 5,6-dimethylbenzimidazole(1) and symmetrically-connected N-heterocyclic carbenes(NHC)[(3a-3c)] were synthesized. Then, the NHC precursor compounds were reacted with PdCl2 and Pd(II)-NHC complexes[(4a-4c)] were obtained. The synthesized NHC precursors(3a-3c) and Pd(II)-NHC complexes(4a-4c) were characterized by different spectroscopic methods. The antibacterial activities of these products were measured against bacteria and fungus with the disc diffusion method. Pd(II)-NHC complexes had higher antibacterial activity than the NHC precursors. The synthesized compounds showed antimicrobial activity with different properties from each other. In vitro biological activities of salts and metal complexes on selected bacteria were determined by the broth dilution method based on Clinical and Laboratory Standards Institute guidelines. 1,3-Bis-(2-hydroxyethyl) imidazolinium bromide and 3-(2-ethoxy-2-oxoethyl)-1-(3-aminopropyl)-1H-imidazole-3-ium bromide had activity against Escherichia coli.en_US
dc.description.sponsorshipTrakya University Research Fund [TUBAP-2014-106]en_US
dc.description.sponsorshipAcknowledgementsThis work was supported by the Trakya University Research Fund(No. TUBAP-2014-106).en_US
dc.identifier.doi10.1007/s40242-023-2355-3
dc.identifier.endpage975en_US
dc.identifier.issn1005-9040
dc.identifier.issn2210-3171
dc.identifier.issue6en_US
dc.identifier.scopus2-s2.0-85161434356en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage968en_US
dc.identifier.urihttps://doi.org/10.1007/s40242-023-2355-3
dc.identifier.urihttps://hdl.handle.net/20.500.14551/22718
dc.identifier.volume39en_US
dc.identifier.wosWOS:001003334500002en_US
dc.identifier.wosqualityN/Aen_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherHigher Education Pressen_US
dc.relation.ispartofChemical Research In Chinese Universitiesen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectN-Heterocyclic Carbeneen_US
dc.subjectPalladium(II)-NHC Complexen_US
dc.subjectStructural Analysisen_US
dc.subjectAntimicrobial Activityen_US
dc.subjectN-Heterocyclic Carbeneen_US
dc.subjectCrystal-Structureen_US
dc.subjectPt(Ii) Complexesen_US
dc.subjectPalladiumen_US
dc.subjectNanoparticlesen_US
dc.subjectAnticanceren_US
dc.subjectLigandsen_US
dc.subjectHecken_US
dc.subjectNhcen_US
dc.titleSynthesis, Spectral Analysis and Antimicrobial Activity of New Pd(II) Complexes Involving 5,6-Dimethylbenzimidazoleen_US
dc.typeArticleen_US

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