Determination of Several Element Levels in Hardaliye Beverages Using Flame Atomic Absorption Spectrometry After Ultrasound-Probe Extraction

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dc.authoridBakircioglu Kurtulus, Yasemin/0000-0003-3013-5793
dc.authoridBakircioglu, Dilek/0000-0003-3384-0340
dc.authorwosidBakircioglu Kurtulus, Yasemin/Q-2570-2017
dc.authorwosidBakircioglu, Dilek/Q-2648-2017
dc.contributor.authorBakircioglu, Dilek
dc.contributor.authorTopraksever, Nukte
dc.contributor.authorKurtulus, Yasemin Bakircioglu
dc.date.accessioned2024-06-12T11:18:57Z
dc.date.available2024-06-12T11:18:57Z
dc.date.issued2017
dc.departmentTrakya Üniversitesien_US
dc.description.abstractIn the present study, concentrations of calcium (Ca), copper (Cu), magnesium (Mg), manganese (Mn), sodium (Na), and zinc (Zn) in hardaliye samples produced in Turkey were determined by flame atomic absorption spectrometry after ultrasound probe extraction (UPE), microwave-assisted extraction (MAE), and wet extraction procedures. At present, there is limited work in the literature on UPE for the determination of trace elements in beverage samples. Our single-correlation analysis showed that the elements studied with the UPE method in hardaliye were strongly correlated with the MAE procedure. The parameters affecting the UPE experimental conditions such as ultrasound amplitude, sonication time, sample amount, extractant type, and volume were studied. Optimal experimental conditions for the extraction of the metals with the UPE procedure were as follows: 2 min of sonication; 30% amplitude; 3 mL sample volume; 5% HNO3 extraction solution; and 1 mL extractant volume for Ca, Cu, Mg, Mn, Na, and Zn in the hardaliye samples. The results in the hardaliye samples in minimum maximum mg/L with the UPE procedure were 33-63 for Ca, 0.10-0.27 for Cu, 3.9-14.4 for Mg, 1.0-3.2 for Mn, 32-58 for Na, and 0.39-1.1 for Zn. LODs were 0.0032, 0.012, 0.013, 0.009, 0.011, and 0.008 mg/L for Ca, Cu, Mg, Mn, Na, and Zn, respectively. The accuracy of the method was verified with a recovery test (in which recoveries between 95 and 110% were observed) and application to a NIST 1643e certified sample (trace elements in water). The UPE procedure was found to be fast, accurate, and simple, with fewer contaminants and lower concentrated reagent consumption in comparison with conventional extraction procedures.en_US
dc.description.sponsorshipTrakya University Scientific Research Projects Commission, Edirne, Turkey [TUBAP-2015-43]en_US
dc.description.sponsorshipThis research was financially supported with funds from the Trakya University Scientific Research Projects Commission (TUBAP-2015-43), Edirne, Turkey.en_US
dc.identifier.doi10.5740/jaoacint.17-0117
dc.identifier.endpage1538en_US
dc.identifier.issn1060-3271
dc.identifier.issn1944-7922
dc.identifier.issue5en_US
dc.identifier.pmid28917262en_US
dc.identifier.scopus2-s2.0-85029469175en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage1531en_US
dc.identifier.urihttps://doi.org/10.5740/jaoacint.17-0117
dc.identifier.urihttps://hdl.handle.net/20.500.14551/25011
dc.identifier.volume100en_US
dc.identifier.wosWOS:000411552000039en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.language.isoenen_US
dc.publisherAoac Inten_US
dc.relation.ispartofJournal Of Aoac Internationalen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectFruit Juicesen_US
dc.subjectAssisted Extractionen_US
dc.subjectIcp-Msen_US
dc.subjectEnvironmental-Samplesen_US
dc.subjectEmission-Spectrometryen_US
dc.subjectTraceen_US
dc.subjectDigestionen_US
dc.subjectMetalsen_US
dc.subjectReden_US
dc.subjectWinesen_US
dc.titleDetermination of Several Element Levels in Hardaliye Beverages Using Flame Atomic Absorption Spectrometry After Ultrasound-Probe Extractionen_US
dc.typeArticleen_US

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