THE Pd(II) COMPLEX INVOLVING A NEW PYROLE-BASED LIGAND: SYNTHESIS, SPECTRAL ANALYSIS, AND ANTIMICROBIAL ACTIVITY

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dc.contributor.authorBoz, Mesut
dc.contributor.authorTetik, Ovul
dc.contributor.authorAltun, Ozlen
dc.date.accessioned2024-06-12T11:03:11Z
dc.date.available2024-06-12T11:03:11Z
dc.date.issued2022
dc.departmentTrakya Üniversitesien_US
dc.description.abstractIn the current study, firstly, a new pyrrole-based ligand (3,4-(ethylenedimercaptodiacetoxy)-N-(benzyl)-diethyl-2,5-pyrroledicarboxylate (L) was synthesized in the presence of diethyl-N-benzyl-3,4-dihydroxy-1H-pyrrole-2,5-dicarboxylate and 2,2'-(ethane-1,2-diylbis(sulfanediyl))diacetylchloride. Then, the palladium(II) complex of the synthesized ligand was obtained, and its structural features were examined by spectral (HRMS, ESI-MS, UV-Visible, FTIR, H-1 NMR, C-13 NMR, XRD-POWDER, SEM, EDX) and thermogravimetric (TG-DTA) techniques. The spectral and thermal measurements of the ligand and its Pd(II) complex show that the ligand is coordinated to the Pd2+ ion. Antimicrobial activities of both the ligand and its palladium complex were examined. It was determined that whereas the ligand indicated modest antimicrobial activity against Staphylococcus aureus and Candida albicans at a concentration of 6.25 mu g/ml, the palladium complex was significantly effective against C. albicans at a concentration of 6.25 mu g/ml.en_US
dc.description.sponsorshipTrakya University; Trakya University. Research Fund (TUBAP) [2017/07]en_US
dc.description.sponsorshipThis study was financially supported by Trakya University. Research Fund (TUBAP, project #2017/07).en_US
dc.identifier.doi10.20450/mjcce.2022.2526
dc.identifier.issn1857-5552
dc.identifier.issn1857-5625
dc.identifier.issue2en_US
dc.identifier.scopus2-s2.0-85147782702en_US
dc.identifier.scopusqualityQ4en_US
dc.identifier.urihttps://doi.org/10.20450/mjcce.2022.2526
dc.identifier.urihttps://hdl.handle.net/20.500.14551/21564
dc.identifier.volume41en_US
dc.identifier.wosWOS:000892492400002en_US
dc.identifier.wosqualityQ4en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherSoc Chemists Technologists Madeconiaen_US
dc.relation.ispartofMacedonian Journal Of Chemistry And Chemical Engineeringen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectHeterocyclic Compoundsen_US
dc.subjectPalladium(II)en_US
dc.subjectSpectral Characterizationen_US
dc.subjectBiological Activityen_US
dc.subjectPt(Ii) Complexesen_US
dc.subjectPalladium(Ii)en_US
dc.subjectPlatinum(Ii)en_US
dc.subjectNanoparticlesen_US
dc.titleTHE Pd(II) COMPLEX INVOLVING A NEW PYROLE-BASED LIGAND: SYNTHESIS, SPECTRAL ANALYSIS, AND ANTIMICROBIAL ACTIVITYen_US
dc.typeArticleen_US

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