Coliform bacteria immobilized on titanium dioxide nanoparticles as a biosorbent for trace lead preconcentration followed by atomic absorption spectrometric determination

Küçük Resim Yok

Tarih

2011

Dergi Başlığı

Dergi ISSN

Cilt Başlığı

Yayıncı

Springer Wien

Erişim Hakkı

info:eu-repo/semantics/closedAccess

Özet

Coliform bacteria physically immobilized on titanium dioxide nanoparticles can be used as a biosorbent for solid phase extraction of lead (II) ions from aqueous solution using a flow injection system coupled to flame atomic absorption spectrometry (FAAS). Effects of pH value, sample volume, flow rates of loading and elution, and the type and volume of eluent were investigated. Lead ions were sorbed on a biosorbent mini-column at pH 6.0, eluted with 1 mol L-1 HCl and then determined by FAAS. The limit of detection for the water samples is in order of 0.90 mu g L-1. The accuracy of the method was confirmed by analyzing a certified reference material (GBW 07605; tea). The results are in good agreement with the certified value. The precision of the method was also satisfactory. The procedure was applied to the evaluation of lead ions in river water, wine, and baby food.

Açıklama

Anahtar Kelimeler

Coliform Bacteria, Titanium Dioxide, Biosorption, Lead, Flow Injection, Solid-Phase Extraction, Amberlite Xad-4, Emission-Spectrometry, Biosorption, Samples, Nickel, Water, Cobalt(Ii), Separation, Iron(Iii)

Kaynak

Microchimica Acta

WoS Q Değeri

Q1

Scopus Q Değeri

Q1

Cilt

174

Sayı

3-4

Künye