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Öğe Adhesion and Surface Roughness of Apatite-Containing Carbomer and Improved Ionically Bioactive Resin Compared to Glass Ionomers(Mdpi, 2023) Isik, Handan Yildirim; Cilingir, AylinThe surface roughness of different glass-ionomer-based materials and their shear bond strength with a resin composite with and without thermal cycling were evaluated. Ketac Molar (KM, 3M ESPE, St. Paul, MN, USA), Glass Carbomer (GC, GCP Dental, Leiden, The Netherlands), Bioactive (BA, PULPDENT, Corporation, Watertown, MA, USA) and Fuji II LC (FJ, GC, Tokyo, Japan) were used to prepare the specimens and they were kept in distilled water at 37 & DEG;C for 24 h. The surface roughness of the specimens was measured with a profilometer (n = 6). A universal adhesive resin was applied on glass-ionomer materials and cylindrical universal composites were applied and polymerized, respectively (n = 16). The specimens were divided into two subgroups. The first subgroup was subjected to thermal cycling. Shear bond strength was investigated for both subgroups (n = 8). Stereomicroscopy and SEM examinations were performed. The roughest surface was obtained in the GC group (p < 0.05). The shear bond strength of the specimens without thermal cycling was higher than that of those with thermal cycling (p < 0.05). The lowest shear bond was measured in the GC group (p < 0.05). Although FJ, KM and BA have been observed to be suitable materials for clinical use, BA, in particular, is evidenced to become the best option among the materials we tested. GC cement's long-term performance needs to be improved.Öğe Adhesion of conventional and self-adhesive resin cements to indirect resin composite using different surface conditioning methods(Taylor & Francis Ltd, 2017) Cilingir, Aylin; Bilhan, Hakan; Cilingir, Altug; Gomec, Yavuz; Ozcan, MutluThis study evaluated the adhesion of conventional and self-adhesive resin cements to indirect resin composite (IRC) using different surface conditioning methods. Cylindrical IRC specimens (N=192) were randomly assigned to four surface conditioning methods (n=8 per group): (a) Control group, (b) Hydrofluoric acid, (c) Tribochemical silica-coating, and (d) 50m Al2O3 air-abrasion. Specimen surfaces were finished using silicon carbide papers up to 600 grit under water irrigation, rinsed and dried. Direct composite blocks were bonded to IRC specimens using three conventional resin cements (Multilink, Panavia F2.0, and Resicem) and three self-adhesive resin cements (RelyX U100, Gcem, Speed Cem). Specimens were subjected to shear bond strength test in a Universal Testing Machine (0.5mm/min). Failure types were categorized as mixed, adhesive and cohesive. Data were analyzed using 2-way ANOVA and Tukey's tests. Two-parameter Weibull modulus, scale (m) and shape (0) were calculated. The bond strength results (MPa) were significantly affected by the surface conditioning method (p<0.0001) and cement type (p<0.001). For Panavia F2.0, Resicem, air-abrasion with 50m Al2O3 significantly increased the results (22.6 +/- 6.5, 26.2 +/- 6.5, respectively) compared to other conditioning methods (13.6 +/- 1.4-21.9 +/- 3.1) but for Multilink, hydrofluoric acid etching (20.5 +/- 3.5) showed significantly higher results (p<0.01). For the self-adhesive resin cements, air-abrasion with 50m Al2O3 significantly increased the results compared to other conditioning methods, except for RelyX U100 (p<0.05). After air-abrasion with Al2O3, Gcem, (11.64), RelyX U100 (9.05), and SpeedCem (8.29) presented higher Weilbul moduli. Exclusively cohesive failure in the IRC was observed with RelyX U100 and Speedcem after Al2O3 air-abrasion.Öğe Color match evaluation using instrumental method for three single-shade resin composites before and after in-office bleaching(De Gruyter Poland Sp Z O O, 2023) Cilingir, Aylin; Kariper, EnginThe aim of this study is to evaluate the effect of an office bleaching agent on the color of various single-shade resin composites. Three single-shade resin composites were tested in this study. Thirty disk-shaped specimens were prepared with a diameter of 10 mm and a height of 1 mm, and they were divided into three groups (n = 10). After color measurements, 40% hydrogen peroxide containing bleaching agent gel was applied to all the specimens. Baseline and final color measurements were performed using a clinical spectrophotometer. Statistical analyses were performed. All bleached specimens had clinically incomprehensible color changes (?E < 3.3). Comparisons for single-shade composites revealed no statistically significant color difference between groups. With the limitation of this study in mind, color changes in single-shade resin-composites after office bleaching were found to be clinically acceptable. It may be appropriate to use single-shade composites that shorten the in-chair clinical time by facilitating shade selection.Öğe Color Stability of Composites After Short-term Oral Simulation: An in vitro Study(Bentham Science Publ Ltd, 2016) Ozdas, Didem Oner; Kazak, Magrur; Cilingir, Aylin; Subasi, Meryem Gulce; Tiryaki, Murat; Gunal, SolenBackground: Although most of the studies investigated color stability of different restorative materials, evaluation of color stability of composites after immersion in multiple beverages in the same day by an in vitro oral simulation study is unclear. Objective: To assess color change of different restorative materials at the end of days 1, 14, and 30 of immersion in multiple liquid types to mimic the oral environment in vitro. Method: Ten disc-shaped specimens were made from each of four different resin composites (Filtek Z250, Voco x-tra base, Beautifil Flow Plus, Beautifil II). Baseline color value of each sample was measured using a spectrophotometer. Each composite was respectively immersed in coffee, an orange/pomegranate juice mixture, black tea, and a mouth rinse on the same day to mimic daily liquid consumption of individuals. Color measurements were taken after 1, 14, and 30 days by spectrophotometer and color change values were calculated. Statistical analyses were executed by one-way ANOVA/Tukey HSD and repeated-measures ANOVA. Results: All materials showed significant color change after 1, 14, and 30 days (P < 0.01) of immersion in liquids, with the lowest color alteration observed at the 1st day and the highest observed after the 30th day. Among the materials tested, at each time point (1, 14, and 30 days), the lowest color alteration was detected in Filtek Z250 and the highest color alteration was detected in Beautifil II. Conclusion: Color alteration of composite resins is affected by composite type and storage time. With the exception of 1 day of storage, color changes of all materials were substantial and clinically unacceptable.Öğe Effect of desensitizers on the microleakage of previously restored Class V resin composite restorations(Taylor & Francis Ltd, 2016) Ozsoy, Alev; Eren, Meltem Mert; Gurbuz, Ozge; Dikmen, Benin; Cilingir, Aylin; Erdemir, UgurObjectives: The aim of this in vitro study was to evaluate the effect of different desensitizers' application on the microleakage of previously restored Class V composite resin restorations. Materials and methods: Class V cavities were prepared on the buccal surfaces of 40 extracted human third molars. Forty box-shaped cavities were divided into four groups, based on the desensitizers used (n = 10). All teeth were restored with the same bonding agent and composite material. No desensitizer was applied in the control group. In the experimental groups, BisBlock, Gluma and Universal bonding agents were the desensitizers. The desensitizers were applied after completion of composite restorations according to manufacturers' instructions. All specimens were then thermocycled at 5-55 degrees C, with a 10-s dwell time for 500 cycles. The samples were then immersed in 0.5% methylene blue dye for 24 h, sectioned into two equal halves, evaluated for microleakage using a stereomicroscope at 30x magnification and scored on a scale of 0-3. The data were analysed using the Kruskal-Wallis test at the significance level p < 0.05. Results: There were no significant differences in microleakage after desensitizer application (p > 0.05). However, based on the obtained numerical values in our study, while the BisBlock and bonding groups showed lower microleakage at the occlusal margin, BisBlock, Gluma and bonding group showed lower microleakage at the gingival margin compared to the control group. Conclusions: The application of desensitizers as a post-treatment option could be considered an advisable procedure to minimize microleakage.Öğe Effect of Different Antioxidants on the Microtensile Bond Strength of an Adhesive System to Sodium Hypochlorite-treated Dentin(Quintessence Publishing Co Inc, 2015) Dikmen, Benin; Gurbuz, Ozge; Ozsoy, Alev; Eren, Meltem Mert; Cilingir, Aylin; Yucel, TanerPurpose: To evaluate the effects of different antioxidant treatments on the microtensile bond strength of an adhesive system to sodium hypochlorite (NaOCl)-treated dentin. Materials and Methods: Thirty extracted third molars were sectioned 3 mm below the occlusal surface and divided into six groups according to the antioxidant treatment received: control group: distilled water; NaOCl group: 5.25% NaOCl and distilled water; proanthocyanidin (PA) group: 5.25% NaOCl, 5% PA and distilled water; 1-week storage group: 5.25% NaOCl and storage for 1 week in distilled water; Accel group: 5.25% NaOCl, Accel, and distilled water; noni group: 5.25% NaOCl, noni fruit juice, and distilled water. NaOCl, PA, Accel, noni, and distilled water were administered for 30 s, 10 min, 30 s, 10 min, and 30 s, respectively. A self-etching adhesive system (Single Bond Universal Adhesive) was applied to each specimen and a resin composite (Filtek Z550) was built up to a height of 5 mm on the dentin surface. Each specimen was serially sectioned to obtain sticks with a cross-sectional area of 1 mm(2), and their microtensile bond strength was determined. Statistical differences between groups were analyzed using one-way ANOVA and Tamhane's T2 test. Results: Microtensile bond strength in the NaOCl group was significantly lower than in all other groups. However, there were no significant differences in the bond strength between the groups treated with different antioxidants. Conclusions: NaOCl significantly reduced the microtensile bond strength of the adhesive system. The application of PA, Accel, and noni fruit juice to NaOCl-treated dentin significantly improved the microtensile bond strength.Öğe Effect of different polishing techniques for composite resin materials on surface properties and bacterial biofilm formation(Elsevier Sci Ltd, 2019) Kurt, Aysegul; Cilingir, Aylin; Bilmenoglu, Caglar; Topcuoglu, Nursen; Kulekci, GuvenObjectives: Both direct and indirect techniques are used for composite resin material (CRM) restorations. Polishing processes are needed in both techniques after intraoral adjustment. However, it is unclear as to which polishing technique should be preferred with respect to decreasing biofilm. The purpose of this in vitro study was to evaluate the surface properties and Streptococcus mutans biofilm formation on direct and indirect CRMs after using different polishing techniques. Methods: Two CRMs (direct and indirect) and four polishing techniques (aluminium oxide discs, diamond polishing paste, aluminium oxide polishing paste, and silicon carbide brush) were evaluated. The specimens were prepared for taking scanning electron microscopy images (n = 2) and determining surface roughness, surface free energy, and bacterial biofilm formation (BBF) with colony-forming unit counting and confocal laser scanning microscopy assays (n = 7). The data were analysed using two-way analysis of variance with Bonferroni as a post hoc test and Pearson's correlation (p < .05). Results: The surface roughness values in the control group were higher than those in the diamond polishing paste group (p = 0.025), but the values in the aluminium oxide polishing paste and silicon carbide brush groups were comparable with those in the control group (p = 0.156 and p = 1.000, respectively). The highest surface free energy values were recorded in the silicon carbide brush group (p < 0.001), whereas there were no differences found among the other groups (p > 0.05). The highest BBF was seen in the silicon carbide brush (p < 0.001) and direct CRM (p < 0.001) groups. Conclusion: BBF on the surface of direct CRMs differed from that on indirect CRMs after polishing the surface. The tested polishing techniques significantly influenced surface properties and BBF. Clinical significance: In situations that require the intraoral adjustment of CRMs, polishing with a diamond polishing paste seems to be a good option to polish the surface of both direct and indirect CRMs because the diamond polishing paste results better in terms of decreasing biofilm formation and improving surface properties.Öğe Effect of surface sealant on the surface roughness of different composites and evaluation of their microhardness(Istanbul Univ Press, Istanbul Univ Rectorate, 2020) Gurbuz, Ozge; Cilingir, Aylin; Dikmen, Benin; Ozsoy, Alev; Eren, Meltem MertPurpose The aim of this study was to evaluate the effect of a surface sealant on the surface roughness of different composites and compare their microhardness values. Materials and Methods Sixty disc-shaped specimens were prepared and assigned to 6 groups (n = 10). Groups were prepared as follows; Group 1 (Herculite XRV Ultra), Group 2 (Beautifil Bulk Restorative) and Group 3 (Filtek Bulk Fill Posterior Restorative). Groups 4, 5, and 6 were prepared by applying a surface sealant (BisCover LV) on the specimens in groups 1, 2 and 3. Surface hardness of the discs in group 1, 2, and 3 and surface roughness of the discs in all groups were measured using the Vickers hardness test and a profilometer, respectively. One-way ANOVA was used to test for differences among the groups. Results No significant differences were observed in the microhardness and roughness between the experimental and control groups for each restorative materials. Group 3 showed the highest surface hardness and group 4 showed the lowest surface roughness values. Conclusion Using the BisCover LV resin after the polishing step has no significant effect on the surface roughness. The highest hardness values were obtained for the Filtek Bulk Fill Posterior Restorative after the polishing step. The smoothest surfaces were obtained for all experimental groups using the BisCover LV resin after the polishing step, Herculite XRV Ultra showed lower average roughness values than the other materials.Öğe The effects of nutritional habits on leucite-based ceramic repaired with nanohybrid composites(Taylor & Francis Ltd, 2019) Kazak, Magrur; Subasi, Meryem Gulce; Ozdas, Didem Oner; Zorlu, Sevgi; Cilingir, Aylin; Gunal, SolenThe purpose of the present in vitro study was to evaluate the effects of nutritional habits (various liquids) on the color change and early repair bond strength of a leucite-based ceramic repaired with different contents of nanohybrid composite resins currently used by the clinicians. Ninety-six IPS-Empress CAD ceramic samples were obtained with low-speed diamond saw. For all samples same repair method was performed. Samples were divided into groups according to four nanohybrid composite resins used as a repair material: Tetric-N-Ceram Bulk Fill, Filtek Z550, Clearfil-Majesty Esthetic, Bisco-Aelite Aesthetic Enamel (n = 24). Composite resins were applied on ceramic surface and polymerized (40 sec). After waiting for 24 h, samples were divided into three subgroups according to liquid types: pomegranate-flavored mineral water, salad dressing, and distilled water (n = 8). Before and after immersion the samples in the various liquids, color measurements were calculated (24 h). Then, shear bond strength was tested with an universal testing machine.For the statistical analyses two-way ANOVA, Tukey HSD, Spearman's correlation tests were used at a significance of p <= 0.05. Nanohybrid composites, liquids (p <= 0.001); correlation between nanohybrid composites and liquids (p <= 0.006) had statistically significant impacts on the color change values. Nanohybrid composites (p <= 0.017) and correlation between nanohybrid composites and liquids (p <= 0.004) had statistically significant impacts on the shear bond strength values. There was not any statistically significant correlation between color change and shear bond strength (p > 0.05). When a composite resin is selected as a repair material, nutritional habits of the patient should be taken into consideration. Although hydrophilic monomer type of a composite material is a more predominant factor associated with color change, filler weight has the same predominant effect on shear-bond strength.Öğe Microleakage Evaluation of Expired and Non-expired Resin Composites and Bonding Agents: In Vitro Study(Sage Publications India Pvt Ltd, 2022) Cilingir, Aylin; Dulger, KivancAim: Although the shelf life is a key property of dental composites and bonding agents, these materials may often be used in simple procedures after expiration. In this study, the microleakage of two year expired and non-expired dental composites (Filtek Ultimate Universal A2 Enamel, 3M ESPE, USA, and Tetric N Ceram A2, Ivoclar Vivadent, Schaan, Liechtenstein) and a universal bonding system (Single Bond Universal, 3M ESPE, USA) was examined. Materials and Methods: In 40 freshly extracted human molars, two standardized Class II cavities (buccolingual and mesiodistal width of 3 mm and 4 mm, respectively) were prepared (80 cavity preparations). The teeth were thermocycled in distilled water for 1000 cycles in a 5 degrees C to 55 degrees C water bath. Next, the teeth and their apical foramens were coated with water resistant nail varnish, except for 1 mm around the restoration-tooth interface, and retained in a 1% methylene blue solution. After 24 h, the specimens were cut into two halves and analyzed using a stereomicroscope. Scanning electron microscopy images of two samples of the groups were obtained. Results: The Kruskal-Wallis test indicated no significant differences between the groups (P < .05). The occlusal median scores were not significant (P = .99). Moreover, the gingival median scores were not significant (P = .48). No difference was found between the occlusal and gingival values in any group (P > .05). Conclusion: These findings indicated that two-year-expired dental composites and bonding agent, which were maintained under proper conditions, do not have any significant difference in terms of the microleakage.